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The patent proprietor regarded the prior art publication on the "building of a water pipe" as demonstrating that a method of making PE pipes with an ultimate strength of 5 MPa and with a slow crack propagation resistance of at least 1000 hours had been known for a long while and was a matter of common and everyday knowledge. Thus, the number of 1000 hours was used for defining the slow crack propagation resistance of PE pipes in application D11 because that was the way it was defined in the standard. The patent proprietor did not regard the fact that the definition of one single property was not consistent throughout this field of application as altering the scope of the claims or as requiring any new test method. This basic classification of slow crack propagation resistance that was reflected in the patent was considered to be sufficient for the standardisation of PE pipes.
Each of the two samples 20/100 and 50/100 from the D11 project (December 1987) tested with regard to slow crack propagation resistance showed a very good level of resistance with values of respectively 1035 and 1130 hours. In addition it was shown experimentally that the ultimate strength of PE increased with increasing PVC content in the range 10 to 80 wt. % and that any further increase in the PVC content tended to increase the hardness of the PVC/PE material to such an extent that it was not possible to make the desired PVC/PE compositions in the required form in a continuous extrusion line. This increase in hardness remained even when increasing the softening effect by means of the addition of the above-mentioned antioxidants.
The patent proprietor finally deduced from the prior art that in order to achieve a property combination of slow crack propagation resistance of at least 1000 hours and ultimate strength of 5 MPa, the use of an ethylene-alpha-olefin copolymer in combination with LDPE to form an extrudate made wholly or partly of such a material could be considered. It was suggested that the initial working temperature be below 90C, preferably below 80C, in order to obtain a combination of properties. Therefore the claims were broadened in order to take account of this prior art. d2c66b5586
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